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The water solubilities of (−)-menthol β-d-glucoside and (−)-menthol α-d-glucoside were tested. Each compound was dissolved at 20 mg/mL in distilled water. The solution was vortexed for 3 min, held overnight at 25 °C, and centrifuged at 6500g for 10 min. The concentration of each compound in the supernatants was quantitatively analyzed by LC–MS/MS analysis in MRM mode.
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