3.6.2. TGA-DSC-SDT

MS María Zenaida Saavedra-Leos
CL César Leyva-Porras
AT Alberto Toxqui-Terán
VE Vicente Espinosa-Solis
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Thermogravimetric (TGA) and differential scanning calorimetry (DSC) analyses were carried out in a simultaneous TGA-DSC SDT Q600 (TA Instruments, New Castle, DE, USA). For the DSC, baseline was calibrated with indium (melting temperature of 156.6 °C and melting enthalpy of 28.47 J/g). Samples of 10 mg were encapsulated in standard aluminum pans. Thermograms were recorded at a heating rate of 5 °C/min over a range of 25–400 °C using Universal Analysis 2000© software.

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