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Prepared according to General Method A to provide material consistent with prior reports38. 15.0 mg (7%); mottled tan powder; 1H NMR (DMSO): 12.35 (br, 1H), 8.08–8.01 (m, 4H), 7.65 (d, 2H), 7.47 (t, 2H); LC/MS: 318.0 (M + 1); mp: >240 °C (decomp.); Rf: 0.25 (50% EtOAc/hexanes).
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