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All the working electrodes were removed from the solution after 13 days, rinsed three times with 1X PBS, fixed with 2.5% glutaraldehyde in PBS for 30 min, then washed twice with high purity water. The specimens were dehydrated in an ethanol series (25%, 50%, 75%, 90% and 100%) for 10 min each and then dried in a biohazard cabinet prior to SEM-EDX analysis.
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Published by the Royal Society under the terms of the Creative Commons Attribution License http://creativecommons.org/licenses/by/4.0/, which permits unrestricted use, provided the original author and source are credited.
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