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The photocatalytic activity of the MoO3-incorporated ZnO nanostructures was tested by photodegradation of rhodamine B (RhB) dye in aqueous solution under visible light irradiation using the same experimental degradation procedure as reported in previous work [3]. Briefly, 5 mg of the catalyst was dispersed in a vial containing 10 mL of RhB dye solution (5 mg/L), having a controlled temperature at 25 °C. A 100 W tungsten lamp was served as the light source. The power of light source was 102.74 kJ·m−2·h−1, and measured by a PMA 2100 apparatus, prod by Solar Light Co. (Glenside, PA, USA). The wavelength range of the tungsten bulb varies between 350 and 850 nm. The initial concentrations of RhB dye and after irradiation at different times were determined using a UV–vis spectrometer SPECORD 210Plus, Analytik Jena (Jena, Germany).

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