PI based on 4,4′-(9-fluorenylidene)dianiline and 3,3′,4,4′-diphenyl oxide tetracarboxylic acid has been used [43]. The molecule structure is given in Figure S1. The density of PI was 1.38 g/cm3 [42].
Tris-(methyldiethoxysiloxy)aluminum (below Al-MDES), tris-(methyldiethoxysiloxy)iron (Fe-MDES), tris-(3-aminopropyldiethoxysiloxy)chromium (Cr-MDES), tetrakis-(methyldiethoxysiloxy)zirconium (Zr-MDES), tetrakis-(methyldiethoxysiloxy)hafnium (Hf-MDES) and pentakis-(methyldiethoxysiloxy)niobium (Nb-MDES) have been used as precursors of the dispersed phase of the composites. Precursors were synthesized according to known methods [40]. The structural formulas of the compounds are given in Figure S2.
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