Reagents and standards

NK Noman Khan
SH Satwat Hashmi
AS Amna Jabbar Siddiqui
SF Sabiha Farooq
SS Shahid Ahmed Sami
NB Nageeb Basir
SB Syeda Saira Bokhari
HS Hasanat Sharif
SJ Sanaullah Junejo
HE Hesham R. El-Seedi
SM Syed Ghulam Musharraf
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During the experimental work, filtered and extremely pure deionized water was obtained from the water filtration and purification system (Thermo scientific, MA USA). Analytical grade reagent (AR, ACS), 70% concentrated HNO3 (RCI Labscan Ltd, Bangkok, Thailand) was used for analysis after purification by NanoPure Acid purification system (Nanonex, USA). Trace metal grade ≥ 30% concentrated H2O2 was acquired from Merck KGaA company (Darmstadt, Germany). The tuning solution with 1 µg/L concentration of Mg, Li, Tl, Y, Co and Ce in 2% HNO3, multi-element calibration solution 2A (Part Number: 8500-6940) with confirmed concentration of 10 µg/mL of each element and, internal standard of 100 µg/mL (Tb, Rh, Ge, Lu, Ir, Bi, and Sc) were bought from Agilent Technologies (Santa Clara, CA, USA). The optimization of ICP-MS parameter was carried out by using tuning solution, before the start of analysis. All cleaned glassware and polypropylene bottles were immersed in 10% (v/v) HNO3 reagent for overnight. After that each apparatus was washed with ultra-pure water three times and kept in laminar-flow hood (Airstream ESCO, Singapore) to dry. The air contamination was prevented by performing experiment in clean hood and working table.

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