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Thermogravimetric (TG) experiments were performed using a TA Instruments Discovery system. Sample powders of about 4–7 mg were heated in a platinum crucible from room temperature up to 750 °C at a heating rate of 5 °C/min and a N2 gas flow of 20 mL/min was applied. Differential scanning calorimetry (DSC) experiments were performed with a Netzsch DSC 214 Polyma instrument from −10 to 300 °C and otherwise using the same conditions as those for the TG experiments.
Copyright and License information: ©2020 American Chemical Society
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