N-(4-Bromophenyl)-2-[4-(3-methoxyphenyl)-2-oxothiazol-3-yl]-acetamide, 9d

CV Claudia Vergelli
IS Igor A. Schepetkin
GC Giovanna Ciciani
AC Agostino Cilibrizzi
LC Letizia Crocetti
MG Maria Paola Giovannoni
GG Gabriella Guerrini
AI Antonella Iacovone
LK Liliya N. Kirpotina
RY Richard D. Ye
MQ Mark T. Quinn
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Yield = 25%; mp = 162-165 °C (EtOH). 1H-NMR (CDCl3) δ 3.83 (s, 3H, CH3); 4.39 (s, 2H, CH2CO); 6.15 (s, 1H, H5-thiazole); 7.01 (s, 3H, Ar); 7.42 (s, 5H, Ar); 8.63 (exch br s, 1H, NH). 13C-NMR (CDCl3) δ 48.8 (CH2); 55.5 (CH3); 99.3 (CH); 114.3 (CH); 116.0 (CH); 116.9 (CH); 121.2 (CH); 121.4 (CH); 130.2 (CH); 131.5 (C); 131.7 (CH); 136.7 (C); 138.3 (C); 159.9 (C); 165.2 (CO); 174.2 (CO). Anal. Calcd for C18H15BrN2O3S (419.29): C, 51.56; H, 3.61; N, 6.68; Found: C, 51.43; H, 3.60; N, 6.72.

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