Magnetic hysteresis measurements were performed using a Quantum Design Magnetic Properties Measurement System (MPMS) at the Brockhouse Institute for Materials Research, McMaster University. Powdered FeOB samples were loaded into gelatin capsules inside a plastic straw with empty capsules above and below the sample to reduce the background contribution from gelatin. Magnetization at 300 K was measured as a function of applied field in the range of +/− 20 kOe and normalized to the sample mass. The GcSi-1 sample was mounted on a quartz rod for measurement. To remove the diamagnetic contribution of the rock substrate, the slope of the high field sections of the hysteresis plot was subtracted from the data set to show the magnetic contribution of the pigment. No mass normalization was performed as the mass of pigment could not be determined without destroying the sample (see SI Text 4, SI Data 3).
Do you have any questions about this protocol?
Post your question to gather feedback from the community. We will also invite the authors of this article to respond.