Improve Research Reproducibility A Bio-protocol resource
- Home
- Protocols
-
Request a Protocol
Ask a
question
Favorite
A sample of compound 2 (5.0 mg) was dissolved in dry pyridine (1.0 mL), and Ac2O (0.5 mL) was subsequently added. After stirring at 40 °C for 48 h, the mixture was concentrated in vacuo to dryness, and the residue was purified by pHPLC with MeCN-H2O (35:65, v/v) at a flow rate of 4 mL/min to yield 2a (1.0 mg). Following the above procedure, compound 12 was acetylated to yield 12a.
Copyright and License information: ©2016, Macmillan Publishers Limited
This work is licensed under a Creative Commons Attribution 4.0 International License. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in the credit line; if the material is not included under the Creative Commons license, users will need to obtain permission from the license holder to reproduce the material. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/
Do you have any questions about this protocol?
Post your question to gather feedback from the community. We will also invite the authors of this article to respond.
Post a Question0 Q&A
