Preparation of the mesoporous zeolite Beta (mBeta)

ZX Zhiguo Xie
XZ Xiaoxia Zhou
HW Huixia Wu
LC Lisong Chen
HZ Han Zhao
YL Yan Liu
LP Linyu Pan
HC Hangrong Chen
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Typically, 0.05 g NaCl and 0.15 g KCl were added into 2 mL distilled water and 14.4 g TEAOH solution. Afterwards, 3.9 g H2SiO3 was dissolved into the above mentioned solution and stirred at 313 K for 6 h. Next, the solution containing 0.033 g NaOH, 0.17 g NaAlO2 and 2 mL distilled water was slowly added into the resultant solution and further stirred at 313 K for 6 h. Finally, 0.5 g CTAB solution was added into the obtained solution and further stirred at 353 K for 8 h. The obtained mixed solution was hydrothermally treated for 48 h at 423 K. Subsequently, the products were washed with distilled water and dried at 383 K for 12 h. The final product mBeta was obtained after calcinations at 823 K for 6 h to remove any organics.

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