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Acetonitrile (HPLC grade), orthophosphoric acid [analytical reagent (AR) grade], sodium hydroxide (AR grade), and ammonium acetate (AR grade) were purchased from E. Merck (India) Ltd. Worli, Mumbai, India. All active pharmaceutical ingredients (APIs) RP, PP, and IP as reference standards were obtained from Medley Pharmaceuticals Limited, Mumbai, India (99.7–99.9% purity).

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