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Micro-focus Raman spectra of different regions (straight, inner regions, middle regions, and outer regions) were collected on a Horiba LabRAM HR Evolution micro-Raman spectrometer with a 600 lines/mm grating and 532 nm laser with the beam size of ~2 μm and accumulated twice with exposing 10 s at each time. In details, a ×50 long working distance Olympus microscope objective was used to focus the laser beam and all the Raman tests are conducted in the room temperature.
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