Differential Scanning Calorimetry (DSC) Analyses

DSC analyses of CMDX, MCDX and RCMDX block copolymers were performed on a TA DSC 2920 calorimeter under nitrogen gas. The solid polymer sample (∼4 mg) was sealed in a hermetic aluminum pan, and an empty hermetic aluminum pan was used as a reference. The samples were heated from 10 to 100 °C at 10 °C/min and then were cooled back to 10 °C at 3 °C/min. Note that the solid polymers were obtained by lyophilization of the corresponding micellar solutions.