NH3-N, NO2−-N, and NO3−-N were determined using UV-Vis spectroscopy analysis, while H2 was detected by the substrate generation-tip collection mode in scanning electrochemical microscopy. The calculations of faradaic efficiency and yield rate were provided in Supporting Information.
Do you have any questions about this protocol?
Post your question to gather feedback from the community. We will also invite the authors of this article to respond.