2.1. Materials

LX Ligang Xu
YW Yali Wang
QL Qunyan Li
SC Suping Cui
MT Mingxue Tang
ZN Zuoren Nie
QW Qi Wei
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Aluminum oxide (Al2O3, 99.99%), starch soluble (98%), methyltrimethoxysilane (MTMS, 98%), hydrochloric acid (HCl, 37%), absolute ethanol (EtOH, 99.9%), polymethyl methacrylate (PMMA, 97%) and methyl tert-butyl ether (MTBE, 99%) were obtained from Fuchen Chemical Reagent Factory (Tianjin, China). Deionized water (H2O) with a resistivity close to 10Ω cm was produced by a water purification system (Ulupure, Chengdu, China). Silica microspheres were home-made according to the references [38,39].

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