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SAXS measurements were conducted in the Materials Characterization Laboratory of the ISIS Neutron and Muon Source, on the Nano-inXider instrument (Xenocs, Sassenage, France) using a microfocus sealed-tube Cu 30 W/30 μm X-ray source (Cu Kα, λ = 1.54 Å). Samples were loaded and gelled in 1 mm path length glass capillary tubes. The q-range investigated was 0.0045–0.37 Å–1, and measurements were made at room temperature.
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