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2.2.4. Hydrolysis and GC–MS Analysis

SV Saúl A. Villafañe-Barajas
MR Marta Ruiz-Bermejo
PR Pedro Rayo-Pizarroso
SG Santos Gálvez-Martínez
EM Eva Mateo-Martí
MC María Colín-García
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To conduct a comparative analysis, a basic (NaOH 0.1N, 100 °C, 6 h) and acid (HCl 6N, 110 °C, 24 h) hydrolysis procedure was performed following previous reports [46,66]. After treatment, the samples (Phases I, II, and III) were analyzed by a GC system coupled to a 5975 VL MSD (Agilent®). The detection and characterization of different signals were performed as previously reported [9,46].

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