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2.3.3. Pilot Production of IPMs

CT Cheng Tang
XC Xiaoming Chen
HY Hua Yao
HY Haiyan Yin
XM Xiaoping Ma
MJ Mingji Jin
XL Xin Lu
QW Quntao Wang
KM Kun Meng
QY Qipeng Yuan
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Icaritin (160 g) was dissolved in 0.2 mol/L sodium hydroxide aqueous solution (8 L) to obtain the base solution of the drug. Soluplus® (640 g), P407 (320 g) and 0.05 mol/L hydrochloric acid aqueous solution (32 L) were added to a glass reactor (50 L) and stirred (1000 rpm) for 2 h. Then, the base solution was pumped into the acid solution over 30 min under stirring (1000 rpm) at 20 °C. IPMs were obtained by centrifugation for 20 min at 10,000 rpm.

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