Improve Research Reproducibility A Bio-protocol resource
- Home
- Protocols
-
Concise Method
4.3.5. Synthesis of Compound 7 (3β,28-lupanediol 28-acetate)
Request a Protocol
Ask a
question
Favorite
To a solution of 4 (3.09 mmol, 1.5 g) in 60 mL mixture of MeOH/THF (2:1 v/v), 10% Pd/C (167 mg) was added and hydrogenated under H2 (40 psi) for 24 h. Next, it was filtered, and the solvent was evaporated under reduced pressure to give 1.49 g, (99+%) as a white crystalline solid.
Copyright and License information: ©2021 by the authors.
Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
Do you have any questions about this protocol?
Post your question to gather feedback from the community. We will also invite the authors of this article to respond.
0/150
Tips for asking effective questions
+ Description
Write a detailed description. Include all information that will help others answer your question including experimental processes, conditions, and relevant images.
Post a Question0 Q&A
