Improve Research Reproducibility A Bio-protocol resource
Concise Method
tooltip

Ethyl 2-Hydroxy-4-(Pyridin-3-Yl)benzoate (15d)

YK Ye Eun Kim
DK Dong Hwan Kim
AC Ami Choi
SJ Seoul Jang
KJ Kwiwan Jeong
YK Young-mi Kim
TN Tae-gyu Nam
ask Ask a question
Favorite

Yellow solid. Yield: 78%. 1H-NMR (400 MHz, CDCl3) δ 11.00 (s, 1H), 8.97 (s, 1H), 8.75 (d, J = 4.9 Hz, 1H), 8.54 (d, J = 7.8 Hz, 1H), 8.03–7.96 (m, 2H), 7.18 (d, J = 1.3 Hz, 1H), 7.08 (dd, J = 8.2, 1.4 Hz, 1H), 4.42 (t, J = 7.1 Hz, 2H), 1.39 (t, J = 7.1 Hz, 3H); 13C-NMR (100 MHz, DMSO-d6) δ 168.65 (s), 160.55 (s), 149.08 (s), 147.40 (s), 143.80 (s), 134.98 (s), 134.20 (s), 130.73 (s), 124.11 (s), 117.99 (s), 115.39 (s), 112.60 (s), 61.45 (s), 13.99 (s); Rf = 0.4 (33% EtOAc in Hex). mp: 162~164 °C (dec.). MS (ESI) m/z 244 [M+H]+. HRMS [M+H]+ C14H14NO3 calcd for 244.0963 found 244.0960.

Copyright and License information:  ©2021 Kim et al.
This work is published and licensed by Dove Medical Press Limited. The full terms of this license are available at https://www.dovepress.com/terms.php and incorporate the Creative Commons Attribution – Non Commercial (unported, v3.0) License (http://creativecommons.org/licenses/by-nc/3.0/). By accessing the work you hereby accept the Terms. Non-commercial uses of the work are permitted without any further permission from Dove Medical Press Limited, provided the work is properly attributed. For permission for commercial use of this work, please see paragraphs 4.2 and 5 of our Terms (https://www.dovepress.com/terms.php).

Do you have any questions about this protocol?

Post your question to gather feedback from the community. We will also invite the authors of this article to respond.

post Post a Question
0 Q&A