Dapoxetine hydrochloride ((S)-N,N-dimethyl-1-phenyl-3-(1-naphthalenyloxy)propanamine hydrochloride, purity ≥ 98%), water (LC–MS grade), β-nicotinamide adenine dinucleotide 2′-phosphate-reduced tetrasodium salt hydrate (NADPH), HLM, sodium phosphate monobasic monohydrate salt and sodium phosphate dibasic anhydrous salt were obtained from Sigma-Aldrich (St. Louis, CA, USA). Acetonitrile (hypergrade for LC–MS) was purchased from Merck (Darmstadt, Germany) and 98% formic acid (MS grade) was obtained from Fluka (Taufkirchen, Germany).

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