Also in the Article



Yellow crystals mp. 118–119 °C, Rf = 0.16 (ethyl acetate:hexan 1:7); 1H NMR (CDCl3, 500 MHz) δ (ppm): 1.26 (s, 3H, C(CH3)2), 1.40 (s, 3H, C(CH3)2), 2.78 (d, 1H, J = 17.3 Hz, CHaHb), 2.96 (d, 1H, J = 17.3 Hz, CHaHb), 4.71 (d, 1H, J = 11.4 Hz, CHI), 6.36 (d, 1H, J = 11.4 Hz, CHAr), 7.48–7.55 (m, 2H, HAr), 7.56–7.61 (m, 2H, HAr), 7.90 (d, 2H, J = 8.2 Hz, HAr), 8.10 (d, 1H, J = 8.6 Hz, HAr); 13C NMR (125 MHz, CDCl3) δ (ppm): 23.6 (C(CH3)2), 32.5 (C(CH3)2), 35.7 (C(CH3)2), 42.5 (CHI), 43.5 (CH2), 77.2 (CHAr), 168.9 (C=O), CAr: 122.9, 124.9, 125.9, 125.9, 126.6, 129.1, 130.2, 131.2, 133.1, 133.9; ESI-TOF HR: m/z calcd for C17H17IO2: 403.0170 [M+Na]+, found 403.0172.

Note: The content above has been extracted from a research article, so it may not display correctly.



Also in the Article

Q&A
Please log in to submit your questions online.
Your question will be posted on the Bio-101 website. We will send your questions to the authors of this protocol and Bio-protocol community members who are experienced with this method. you will be informed using the email address associated with your Bio-protocol account.



We use cookies on this site to enhance your user experience. By using our website, you are agreeing to allow the storage of cookies on your computer.