Also in the Article



Colorless crystals mp. 107–108 °C, Rf = 0.25 (ethyl acetate:hexan 1:7); 1H NMR (CDCl3, 500 MHz) δ (ppm): 1.20 (s, 3H, C(CH3)2), 1.28 (s, 3H, C(CH3)2), 2.61 (d, 1H, J = 17.4 Hz, CHaHb), 2.81 (d, 1H, J = 17.4 Hz, CHaHb), 4.11 (d, 1H, J = 10.8 Hz, CHBr), 5.40 (d, 1H, J = 10.8 Hz, CHAr), 7.35–7.42 (m, 5H, HAr); 13C NMR (125 MHz, CDCl3) δ (ppm): 21.4 (C(CH3)), 29.6 (C(CH3)2), 35.5 (C(CH3)2), 44.0 (CH2), 61.3 (CHBr), 83.3 (CHAr), 168.4 (C=O), CAr: 127.5, 128.5, 129.2, 137.1; ESI-TOF HR: m/z calcd for C13H15BrO2: 305.0153 [M+Na]+, found 305.0138.

Note: The content above has been extracted from a research article, so it may not display correctly.



Also in the Article

Q&A
Please log in to submit your questions online.
Your question will be posted on the Bio-101 website. We will send your questions to the authors of this protocol and Bio-protocol community members who are experienced with this method. you will be informed using the email address associated with your Bio-protocol account.



We use cookies on this site to enhance your user experience. By using our website, you are agreeing to allow the storage of cookies on your computer.