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Colorless crystals m.p. 105–106.5 °C, Rf = 0.18 (acetone:hexan 1:7); 1H NMR(CDCl3, 500 MHz) δ (ppm): 1.25 (d, 3H, J = 6.4 Hz, CH(CH3)), 2.35–2.47 (m, 2H, J = 17.2 Hz, CHaHb), 2.92–3.01(m, 1H, CHaHb), 3.76 (t, 1H, J = 9.8Hz, CHCl), 5.18 (d, 1H, J = 9.8 Hz, CHAr), 7.33–7.43 (m, 5H, HAr); 13C NMR (125 MHz, CDCl3) δ (ppm): 19.6 (CH(CH3)), 35.2 (CH(CH3)2), 37.1 (CH2), 63.3 (CHCl), 85.0 (CHAr), 168.9; (C=O), CAr: 127.51, 128.5, 129.2, 136.4; IR (cm−1): 1730, 1496, 1460, 1401, 1376, 1345, 1288, 1240, 1218, 1184, 1107, 1074, 1055, 1031, 1020, 995, 930, 906, 893, 850, 800, 757, 670, 651, 618;. ESI-TOF HR: m/z calcd for C12H13ClO2: 247.0502 [M+Na]+, found 247.0510.

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