MIL-101(Cr) was hydrothermally synthesized according to the previous procedure [34] using Cr(NO3)3·9H2O (8 g), H2BDC (3.32 g) and deionized water (100 ml). The mixture was stirred for 30 min using a magnetic stirrer. HF (10 mmol) was gradually added to the mixture and stirred for 15 min. The mixture was placed in a stainless-steel Teflon-lined autoclave, sealed and inserted into a preheated electric oven at 483 K for 8 h. Next, the autoclave was allowed to cool to room temperature and the product was filtered and recovered. The as-synthesized product was further purified using deionized water, DMF and ethanol to remove possible impurities in the pores. The product yield reached as high as 89%. The purified product was finally dried overnight, cooled to room temperature and stored in a desiccator.

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