The samples were first dried to a constant weight at 80°C. A small amount of sample powder was attached to the copper platform, and then the sample was sprayed with gold to increase the conductivity of the sample, making the image clear and stable. The gold sprayed samples were placed in a vacuum system in the scanning electron microscope and were vacuumed and scanned. During the test, images were displayed by a computer system, and the results were recorded at resolutions of 10 μm and 2 μm, respectively.

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