Mn-TCPP, MOF or Mn-MOF was suspended in deionized water at Zr concentration of 50 µg/mL and Mn concentration of 10 µg/mL and then incubated with 400 µM H2O2. SOSG at the final concentration of 5 μM was added to the above suspensions and the mixtures were irradiated with US (1 MHz, 0.9 W/cm2, 30% duty cycle) for different time intervals under normoxic (air with about 21% O2) and hypoxic (a closed box filled with nitrogen gas) conditions. The fluorescence was measured by a Fluoromax-Plus spectrofluorometer (Horiba-Jobin Yvon Inc, Edison, NJ, USA) at the excitation and emission wavelength of 488 nm and 525 nm, respectively.

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