Mn-TCPP, MOF or Mn-MOF at Zr concentration of 10 and 20 μg/mL (the corresponding Mn concentration was 2 and 4 μg/mL for Mn-TCPP) was incubated with 5 μM GSH at 37 °C for 40 min. The samples were centrifuged at 15,000 rpm for 10 min and the supernatants were collected for GSH measurement by a GSH assay kit according to the manufacturer's guidance.

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