Single-crystal growth of Pt1Ag28(S-2-Adm)20 and Pt1Ag28(S-2-Adm)18(HO-2-S-Adm)2
This protocol is extracted from research article:
Valence self-regulation of sulfur in nanoclusters
Sci Adv, Nov 22, 2019; DOI: 10.1126/sciadv.aax7863

Nanoclusters were crystallized in a CH2Cl2/ether system with a vapor diffusion method. Specifically, 20 mg of clusters was dissolved in 5 ml of CH2Cl2, and the obtained solution was then vapor-diffused by 50 ml of ether. After 3 days, dark crystals were collected and subjected to XRD to determine the structure.

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