We performed DNP and EPR studies on four different trityl radicals, namely, OX063, deuterated d24-OX063, Finland (37), and perdeuterated d36-Finland (Fig. 1B). The trityl radicals were obtained from GE Healthcare (Amersham, UK). Samples of 5 mM trityl dispersed in a mixture of d8-glycerol:D2O:H2O (60:30:10 by volume), also known as DNP juice, were used in all DNP experiments except for the dilution analysis (Fig. 2B).

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