Preparation of click-ionogels
This protocol is extracted from research article:
Ionic liquid–based click-ionogels
Sci Adv, Aug 23, 2019; DOI: 10.1126/sciadv.aax0648

The preparation method of click-ionogels is similar to AB glue. First, PEGDA (0.6 g, 1 mmol), PETA (43.8 mg, 0.1 mmol), and BTCA (12.7 mg, 0.05 mmol) were thoroughly dissolved in 0.4 ml of methanol to obtain a homogeneous and transparent solution, namely, precursor solution A. Similarly, 50 mg of PIL-BF4, TEA (11 mg, 0.11 mmol), and ED (112.8 mg, 1.2 mmol) were dissolved in 0.4 ml of methanol to obtain a homogeneous transparent solution, namely, precursor solution B. Then, the mixture of precursor solutions A and B (VA/VB = 1) was poured into the mold and the gelation reaction was conducted at room temperature for 3 hours. Subsequently, the obtained gel was soaked in IL-BF4 and then dried at 80°C under vacuum for 24 hours to displace methanol with IL-BF4. The IL content of the click-ionogel is about 53 wt %.

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