Far-field FTIR spectroscopy was collected using the spectrophotometer Agilent model Cary 630 FTIR in ATR geometry using a diamond crystal. The synchrotron radiation XRD was performed at the XRD2 beamline of the LNLS using an energy of 7 keV (λ = 1.7712 Å) in 10° < 2θ < 60°. The detector was a MYTHEN 1K from DECTRIS, mounted on grazing-incidence diffraction. The incidence angle was 4°, and the measurements were performed at room temperature. Materials and Methods should provide sufficient information to allow replication of the results. Begin with a section titled Experimental Design describing the objectives and design of the study as well as prespecified components.

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