The synchrotron radiation XRD measurements under high pressure were performed at GeoSoilEnviroCARS (GSECARS), beamline 13-BM-C of the Advanced Photon Source, Argonne National Laboratory. A monochromatic x-ray beam was used with a wavelength of 0.434 Å. Experimental fitting of synchrotron radiation XRD data was carried out using TOPAS3 (48) in a whole powder pattern fitting approach.

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