XAS measurements were carried out at experimental station 8-2 of the Stanford Synchrotron Radiation Light Source. XAS data were recorded in fluorescence yield mode. ZnxCo1−xO electrodes were processed using CV. After five cycles with the scan rate of 10 mV s−1, the electrode was cycled at 5 mV s−1 to the required potential. The electrodes were then taken out from the electrolyte, washed with ethanol, dried using argon gas, and then sealed in tape to prevent exposure to the environment.

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