The samples were well characterized by measuring x-ray single-crystal diffraction, elemental analysis, electrical resistivity, and thermopower, confirming that our crystals are stoichiometric (22). Our energy-dispersive spectroscopy results reveal an atomic ratio of the samples with Zr:Te ≈ 1:5 (table S2). We also used an FEI Titan Cs-corrected cross-sectional STEM operating at 200 kV to further examine the crystalline nature of the ZrTe5 sample.

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