TFB (97%), BTA, and benzene (anhydrous, 99.8%) were purchased from Sigma-Aldrich, and DMF (anhydrous, 99.8%) was ordered from Thermo Fisher. All the chemicals were used without further purification. Asymmetric α-Al2O3 disks (γ-Al2O3 on top) with a diameter of 18 mm and a thickness of 1 mm were purchased from Fraunhofer Institut für Keramische Technologien und Systeme (IKTS). The average pore size of the top layer is ca. 5 nm.

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