A 25-ml stainless steel autoclave with mechanical stirrer was loaded with 50 mg of catalyst and 10 ml (7.0584 g, 62.9 mmol) of substrate, which was dried over Na and freshly distilled. The autoclave was closed and flushed with H2 three times. H2 (40 bar) was charged, and the autoclave was heated to 150°C with an aluminum block and stirred properly. When the pressure dropped to around 5 bar, it was readjusted to 40 bar. After the denoted reaction time, the autoclave was cooled with an ice bath and the pressure was carefully released. The mixture was filtered through a filter paper into a round bottom flask (6.843 g, 59.9 mmol, 95%). Mesitylene was added as internal standard, and 1H NMR was measured.

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