Synthesis of homoleptic bis(dipyrrinato)zinc(II) complex homopolymer, Homo-2

A methanol solution (2.5 ml) of zinc(II) acetate (0.46 mg, 2.5 μmol) was added to a dichloromethane solution (5 ml) of H2L2 (2.08 mg, 2.0 μmol), and the mixture was stored in the dark. After 4 days, red powdery solid was formed in the reaction mixture, which was collected by filtration, washed with methanol and dichloromethane, and then dried to obtain Homo-2.

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