MoS2 powder was purchased from Sigma-Aldrich (USA). LA, n-butyllithium solution, and DOX hydrochloride were purchased from J&K Chemical Ltd. (Beijing, China). PEG polymers were purchased from Seebio Biotech Inc. (Shanghai, China). All high-performance liquid chromatography–grade solvents were purchased from Beihua Chemicals Inc. (China). Deionized water was purified using a Milli-Q Integral water purification system (Millipore, USA). Multiwalled carbon nanotubes (length, 5 to 20 nm) were purchased from Nanjing XFNANO Materials Tech Co. Ltd. (Nanjing, China). Black phosphorus powder was purchased from Sante Materials Tech Co. Ltd. (Taizhou, China).

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