TA powder (25 g) was added to a vial and then heated at 70°C in an oil bath. A yellow transparent low-viscosity liquid was obtained after 1 min, and then the stirring was started. DIB (5 g, 20 wt %) was injected under stirring, and the mixture was stirred at 70°C for 5 min. Subsequently, a certain amount of FeCl3 [determined by the molar ratio of TA to iron(III)] was added to the mixture under violent stirring. The liquid mixture was then easily poured into the desired mold, and the yellow transparent solid copolymer was obtained after cooling down to room temperature.

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