The GPE was prepared by in situ gelation of a precursor solution in a sealed pellucid glass reagent bottle. The precursor solution consisted of 2 M LiPF6 dissolved in a common DOL/DME LE, which contained 1 M lithium bis(trifluoromethanesulfonyl)imide (LiTFSI) in a mixed organic solution of DOL and DME (1:1 , v/v). The precursor solution spontaneously transformed into GPE by standing for a period of time at room temperature. All processes of preparing the GPE were conducted in an Ar-filled glove box.

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