Different Sor-Tos crystal habits, including ST-A and ST-B, were prepared by recrystallization from acetone and n-butanol, respectively. The mixtures were heated to 60 °C with stirring until the solids dissolved completely, then the solutions were cooled to room temperature and the crystal habits of Sor-Tos were formed. The crystals were then filtered and dried at 50 °C for 2 h. The dried crystals were ground and sieved through a 75 μm sieve.

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