Sorafenib tosylate (purity > 98%) was a kind gift from Eastchina Pharm. Co., Ltd., Zhejiang, China. It was initially characterized by PXRD. Acetone (ACN, MW = 58.08) and n-butanol (BuOH, MW = 74.12) were supplied by Sigma-Aldrich Co., Ltd., Santa Clara, CA, USA. All other materials and solvents were of analytical grade.

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